Introduction: Thyme contains a surprising amount of iron compounds. This audition enables us to determine the amount of iron(II) present in deviate thyme by means of a redox reaction. Method: 1. weigh accurately ab come out of the closet 1g of dried thyme and put into a 250cm3 beaker. submit the mass of thyme used. 2. employ a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) pernicious and boil gently for 5 minutes. 3. Allow the mixture to hush for a few minutes then filter it, victimization either gravity or vacuum filtration. (We shall be development vacuum filtration.) Wash the residue in the funnel at a time with a little water and squirrel away all the filtrate. 4. displace all the filtrate and washings into a 250cm3 volumetric flaskful. Make up to 250cm3 with 1.0mol dm-3 sulphuric venomous(VI) acid. Stopper the flask and chase away several measure to thoroughly mix the solution. 5. Fill the buret with 0.005mol dm-3 potassium manganate(VII) solution. 6. displace some of the thyme extract solution into a 250cm3 plastic beaker. 7. victimisation a measuring cylinder, add 50cm3 of 1.0mol dm-3 sulphuric(VI) acid to the thyme extract in the conical flask. 8. Titrate the solution in the conical flask with the potassium manganate(VII) solution until a grisly pink colouration persists for 10 seconds. 9. Repeat the titration until there be two titres at heart 0.1cm3 of each other.
Record results in a suitable table. Results: close to determineher(p) Titre: 7.653 First slant: 6.553 Second Run: 6.453 trio Run: 6! .553 Calculations: During the titration, iron(II) ions are oxidised to iron(III) ions and manganate(VII) ions are reduced to manganese(II) ions. The equation is as follows: 5Fe2+(aq) + MnO4-(aq) + 8H+(aq) ? 5Fe3+(aq) + Mn2+(aq) + 4H2O(l) The above equation shows that one mole of manganate(VII) ions reacts with 5 moles of iron(II) ions in acid solution. Using our average titre of 6.52cm3 we mustiness first work out how many moles of potassium manganate(VII) are used. Moles in a...If you want to get a full essay, sound out it on our website: OrderCustomPaper.com
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